DISTILLATION
148
Heads
Distillation Head with a Condenser and Medium Length Standard Taper Joints Distillation head with a condenser sealed to the vertical tube • Standard Taper 14/20 outer joint on the vertical tube can be converted to a thermometer joint using the 273500, size 21 bushing adapter • The height of this joint is fixed in relation to the side arm, permitting use of 25 mm immersion thermometers • Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A requirements
Short Path Improved Distillation Head • Excellent for use when distilling solvents with medium to high boiling points • Designed with a combination cold coil and Leibig condenser • Water flows into the middle hose connection through the coil and exits the outer jacket through the top hose connection • Top outer joint is Standard Taper 10/30 for use with a 51 mm immersion thermometer • Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A requirements
Standard Taper Joints
Part Number
Condenser Joint Case Qty
Standard Taper Joint: Lower
Fits Tubing ID (inches)
Part Number
Case Qty
286900-0000
14/20
14/35
1
513810-2440
24/40
0.375
1
Distillation Head with a Condenser and Full Length Standard Taper Joints Distillation head with condenser and full length standard taper joints. • Simple take-off unit with a condenser sealed to the adapter at a 75° angle • With bottom and side Standard Taper inner drip joints • Standard Taper 10/30 outer joint on top accepts a 75 mm immersion thermometer • Hose connections are designed to fit 3/8” ID flexible tubing • Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A requirements
Short Path Improved Vigreux Distillation Head • Excellent for use when distilling solvents with medium to high boiling points • Designed with a combination cold coil and Leibig condenser • Vigreux indentations improve efficiency • Water flows into the middle hose connection and through the coil and exits the outer jacket through the top hose connection • Top outer joint is Standard Taper 10/30 for use with a 51 mm immersion thermometer • Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A requirements
Standard Taper Joints
Thermometer Standard Taper Joint
Part Number
Case Qty
514000-2440
24/40
10/30
1
Standard Taper Joint: Lower
Fits Tubing ID (inches)
Short Path Distillation Head •
Part Number
Case Qty
When a Standard Taper thermometer is inserted in the top of this apparatus, the bulb and stem serve as column packing Close-coupled condenser and vacuum connection offer an extremely short condensate travel path
513850-2440
24/40
0.375
1
•
•
Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A requirements
Vacuum Jacketed Vigreux Distillation Head with Condenser • Distillation head with a condenser sealed to a jacketed Vigreux distilling column • Standard Taper thermometer joint on the top of the vertical column • Vacuum adapter section of this apparatus takes a 287902 distribution adapter and four receiving flasks • Joints may be held with springs or Standard Taper polyacetal clamp • Stabilizing bar runs perpendicularly between vertical column and vacuum adapter • Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A requirements
Standard Taper Joints
Fits Tubing ID (inches)
Part Number
Case Qty
287100-0000 287110-0000 513750-0000 513750-2942
14/20 19/22 24/40 29/42
0.25 0.25
1 1 1 1
0.375 0.375
Short Path Vacuum Jacketed Distillation Head • Vacuum-jacketed design for more efficiency •
When a Standard Taper thermometer is inserted in the top of this apparatus, the bulb and stem serve as column packing
Standard Taper Joints
Fits Tubing ID (inches)
Part Number
Case Qty
• The close-coupled condenser and vacuum connection offer an extremely short condensate travel path • Manufactured from 33 expansion, low extractable borosilicate glass conforming to USP Type I and ASTM E438, Type I, Class A requirements
287320-0000
14/20
0.25
1
Accessories
Standard Taper Joints
Fits Tubing ID (inches)
Part Number 287902-0000
Description
Case Qty
Part Number
Case Qty
Distribution Adapter for 287900
1
287150-0000 513770-0000
14/20 24/40
0.25
1 1
Size 14 Polyacetyl, Standard Taper Clamp, Yellow, Fits joint sizes 14/20, 14/35
675300-0014
12
0.375
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